At present, in R&D Lab, the various reactions at different desired temperatures are done in Glass Round Bottom Flask, using an Oil or Water Bath and Over Head Stirrer.
The problem being faced in above procedure:
DU has introduced Single Station Lab Reactor to overcome the above mentioned problem.
It consists of 1Litre Capacity Reactor Vessel, complete with Control Unit for Continuous Variable Speed Control, PID Temperature Control, Provision for connecting Water Pump motor electrically and 2-Pole MCB for Mains ON/OFF with suitable Glass Fuses and connectors, and mounted over a Trolley.
2Litre & 3Litre Capacity Reactor Vessels complete with Electrical Heater, Jacketing for Cooling, Flush Bottom Valve with Emergency Ball Valve, Stirring Rod with suitable Anchor & Turbine type stirrer blade suitable for Respective Capacities and suitable Stand to mount over the trolley platform respectively.
|1||Nominal Capacity of Reactor Vessel (Litre)||1||2||3|
|2||Total Volume of Reactor Vessel (Litre)||1.5||3||4|
|3||Inner Diameter of Reactor Vessel (mm)||160|
|4||Working Height of Reactor Vessel (mm)||75||150||210|
|5||Jacketing Total Volume (L)||0.065||1.3||2|
|6||Jacketing Effective Volume (L)||0.4||1||1.5|
|7||Max. Operating Temperature (°C)||Ambient + 10°C to 180°C|
|8||Max. positive pressure (bar)||1bar above Atmospheric Pressure|
|9||Negative pressure (vacuum) (mbar)||10 mbar|
|10||Overhead Lab stirrer(LS-5)||60-600RPM (other speed as required)|
|11||Input Supply||230 V, AC, ±10%|
|12||Weight of Trolley Platform with stand and Accessories (Without Reactor Vessel)||108 Kg|
|13||Weight of Reactor Vessels (Kg)||27Kg||29Kg||32Kg|
|14||Reactor Vessel Dimension (W X D X H) (mm) : A X B X C||515x285x920||515x285x920||515x285x980|
|15||Overall dimensions of system (W X D X H) (mm)||900x750x1835|